Advanced Practical Organic Chemistry
The first edition of this book achieved considerable success due to its ease of use and practical approach, and to the clear writing style of the authors. The preparation of organic compounds is still central to many disciplines, from the most applied to the highly academic and, more tan ever is not limited to chemists. With an emphasis on the most up-to-date techniques commonly used in organic syntheses, this book draws on the extensive experience of the authors and their association with...
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The first edition of this book achieved considerable success due to its ease of use and practical approach, and to the clear writing style of the authors. The preparation of organic compounds is still central to many disciplines, from the most applied to the highly academic and, more tan ever is not limited to chemists. With an emphasis on the most up-to-date techniques commonly used in organic syntheses, this book draws on the extensive experience of the authors and their association with some of the world's mleading laboratories of synthetic organic chemistry. In this new edition, all the figures have been re-drawn to bring them up to the highest possible standard, and the text has been revised to bring it up to date. Written primarily for postgraduate, advanced undergraduate and industrial organic chemists, particularly those involved in pharmaceutical, agrochemical and other areas of fine chemical research, the book is also a source of reference for biochemists, biologists, genetic engineers, material scientists and polymer researchers. Booknews A guide to the preparation of organic compounds and types of reactions used in modern organic synthesis, emphasizing recent techniques. Covers lab basics such as safety, record keeping, and equipment, presents techniques for working with solvents, reagents, gases, and vacuum pumps, and details carrying out reactions, purification, and characterization. Includes a review of the chemical literature, and appendices listing properties of solvents, gases, reducing reagents, and oxidizing reagents. For postgraduates and advanced undergraduates. Annotation c. Book News, Inc., Portland, OR (booknews.com)
1General Introduction12Safety33Keeping records of laboratory work84Equipping the laboratory and the bench365Purification and drying of solvents546Reagents: Preparation, purification and handling697Gases1078Vacuum pumps1229Carrying out the reaction12810Working up the reaction17711Purification18412Small scale reactions22713Large scale reactions23614Special procedures24015Characterization25016'Trouble shooting'; what to do when things don't work25817The chemical literature262Appendix 1. Properties of common solvents277Appendix 2. Properties of common gases278Appendix 3. Approximate pKa values for some common deprotonations compared to some common bases279Appendix 4. Lewis acids280Appendix 5. Common reducing reagents281Appendix 6. Common oxidizing reagents285Index289
\ BooknewsA guide to the preparation of organic compounds and types of reactions used in modern organic synthesis, emphasizing recent techniques. Covers lab basics such as safety, record keeping, and equipment, presents techniques for working with solvents, reagents, gases, and vacuum pumps, and details carrying out reactions, purification, and characterization. Includes a review of the chemical literature, and appendices listing properties of solvents, gases, reducing reagents, and oxidizing reagents. For postgraduates and advanced undergraduates. Annotation c. Book News, Inc., Portland, OR (booknews.com)\ \
