Nanophase Materials: Synthesis - Properties - Applications

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Author: George C. Hadjipanayis

ISBN-10: 0792327543

ISBN-13: 9780792327547

Category: Nanostructure materials -> Congresses

Nanophase Materials is the first and, as yet, the only comprehensive book published in this new and exciting area of materials science. It gives a broad overview of the revolutionary new field of nanophase materials; a view which spans the materials, physics, and chemistry research communities at a tutorial level that is suitable for advanced undergraduates, graduate students, postdoctoral researchers, and experts or would-be experts in the science of nanostructured materials. The articles...

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Nanophase Materials is the first and, as yet, the only comprehensive book published in this new and exciting area of materials science. It gives a broad overview of the revolutionary new field of nanophase materials; a view which spans the materials, physics, and chemistry research communities at a tutorial level that is suitable for advanced undergraduates, graduate students, postdoctoral researchers, and experts or would-be experts in the science of nanostructured materials. The articles are authored by many of the world's most prominent scientists in this field. The book covers the diverse methods for synthesizing nanophase materials, a variety of subsequent processing methodologies, what is known about the structures of these materials on various length scales from atomic to macroscopic, and the properties of these unique and novel materials. The materials properties covered are mechanical, electronic, optical, and magnetic and hence span a wide range of important new opportunities for technological applications. Booknews The June-July 1993 NATO ASI covered a broad spectrum of topics from the disciplines of physics, chemistry, biology, and materials science that comprise the new and developing field of nanophase materials. The nature of nanophase materials was discussed in relation to other similar nanostructured materials and the fundamental criteria for their synthesis were elucidated. This volume contains lectures, invited talks, and poster presentations organized into seven chapters: synthesis; characterization; mechanical properties; electronic and transport properties; optical properties; magnetic properties; and applications. Annotation c. Book News, Inc., Portland, OR (booknews.com)

PrefaceChemical Synthesis of Nanophase Materials1Preparation of [actual symbol not reproducible] Particles21Synthesis of III-V Semiconductor Particles from Organometallic Precursors29Synthesis of Nanostructured Catalysts and Catalytic Supports37Formation of Magnetic Spinel Iron Oxide in Solution45Synthesis of Nanoscale Iron Oxide Structures Using Protein Cages and Polysaccharide Networks49Gas Evaporation and Electron Microscopical Observation of Small Particles57Nanoparticles from a Supersaturated Vapor73Formation and Phase Analysis of Surface Oxides on Ultrafine Particles of Fe81[actual symbol not reproducible] Nanophase Powders Prepared by a Vaporization/Condensation Process in a Solar Furnace85Synthesis and Characterization of Iron-Magnesium Bimetallic Particles89Nanometric Si-Based Powders by Laser Driven Gas Phase Reactions93Simulations of Aggregating Particles97Spark Erosion for Production of Nanocrystalline Materials101Aerosol Spray Pyrolysis Synthesis Techniques109Nanometric Si/C/N Composite Powders Formed by Aerosol-Laser Interaction117Preparation of Small Particles of Titanium (IV) Oxide121Nanophase Materials by Mechanical Attrition: Synthesis and Characterization125High-Capacity High-Energy Ball Mill for Nanophase Materials145Ball Velocities and Energy Needs in a Mill Designed for the Synthesis of Nanophase Materials149Production of Nanocrystalline Materials Through the Mechanical Crystallization of Amorphous Precursors153Structure of Nanostructured Materials157High Resolution Microscopy Characterization of Nanostructured Materials181Surface Structure of Nanocrystalline Oxides197STM "Tip Changes" - A Possible Tool for Tip Characterization205The Structural Evolution of Nanocrystalline Thin Films of Germanium209Fabrication and X-ray Photoelectron Spectroscopy of Nanostructured Semiconductor Thin Films and Particles213Optical Characterization of Fractal Aggregate Size and Morphology Parameters221Studies of Oxide Reduction and Gas Adsorption by Using Positron Annihilation Spectroscopy225Mechanical Properties of Nanophase Materials233Nanostructured Ceramics: Microstructure and Properties263Grain Boundary Structure and Mechanical Properties of Nanocrystalline Materials275Microstructure in Nanocrystalline Zirconia Powders and Sintered Compacts283Mechanical Properties of Nanostructure Niobium on a Microscopic Scale287Mechanical Properties of Artificially Multilayered and Granular Metal Thin Films293Elastic Properties of Metallic Multilayers307Molecular Dynamics of Nanophase Intermetallics315Electronic Structure and Total Energy of Crystalline Approximants to Quasicrystalline Al-Cu-Fe Alloys323Melting 1n Restricted Geometries333Thermodynamics of Finite Systems341Electronic Properties of Metal Cluster Compounds: Nanophase-Materials from Chemical Synthesis349Electronic and Structural Properties of Caged Metal Clusters371Electronic Transport in Granular Metal Films381Superconductivity in Nanophase Materials399Morphology and Transport Properties of Nanophases in Semiconductor Multilayer Films407Anisotropic Electron Transport in Metallic Multilayers415Electronic Transport in Nanocrystalline Metals: A Study of Electrodeposited Nickel Foils423Electronic and Optical Properties of Semiconductor Nanocrystals: From Molecules to Bulk Crystals433Optical Properties of Granular Solids449Se EXAFS Study of the Elevated Wurtzite to Rock Salt Structural Phase Transition in CdSe Nanocrystals471Raman Diagnostics of Silicon and Carbon Nanoparticles483Optical and Related Properties of Semiconductors: Bulk and Small Particles493Nanometer Sized Particles of PbI[subscript 2] Layered Semiconductors, Embedded in SiO[subscript 2] Films: Quantum Size Effect and Photodecomposition Processes503Photonic Band Gap Materials509Surface Magnetism of Nanometer Particles515Nanostructural Design of Magneto-Optic Films and Multilayers537Giant Magneto-Transport Properties in Granular Magnetic Systems555Two-Dimensional Patterns of Ni Particles - Preparation and Magnetic Measurements569Magnetism in Ultrafine Fe and Co Particles573Magnetism of Surface-Treated Particles587Amorphous Magnetic Particles595Properties of Co/B Fine Particles Made by the Microemulsion Technique613Magnetic and Optical Properties of [actual symbol not reproducible] Nanocrystals617Size Effects on the Structural and Magnetic Properties of Ultrafine Fe-Pd Particles625Nanostructured Magnetic Materials: Size and Interaction Effects on Magnetic Properties of Fine Particles635Magnetic Relaxation in Interacting Small Iron Particles645

\ BooknewsThe June-July 1993 NATO ASI covered a broad spectrum of topics from the disciplines of physics, chemistry, biology, and materials science that comprise the new and developing field of nanophase materials. The nature of nanophase materials was discussed in relation to other similar nanostructured materials and the fundamental criteria for their synthesis were elucidated. This volume contains lectures, invited talks, and poster presentations organized into seven chapters: synthesis; characterization; mechanical properties; electronic and transport properties; optical properties; magnetic properties; and applications. Annotation c. Book News, Inc., Portland, OR (booknews.com)\ \