Lc/ms: A Practical User's Guide
A practical guide to using and maintaining an LC/MS system\ The combination of liquid chromatography (LC) and mass spectrometry (MS) has become the laboratory tool of choice for a broad range of industries that require the separation, analysis, and purification of mixtures of organic compounds.\ LC/MS: A Practical User's Guide provides LC/MS users with an easy-to-use, hands-on reference that focuses on the practical applications of LC/MS and introduces the equipment and techniques needed to...
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A practical guide to using and maintaining an LC/MS system The combination of liquid chromatography (LC) and mass spectrometry (MS) has become the laboratory tool of choice for a broad range of industries that require the separation, analysis, and purification of mixtures of organic compounds.LC/MS: A Practical User's Guide provides LC/MS users with an easy-to-use, hands-on reference that focuses on the practical applications of LC/MS and introduces the equipment and techniques needed to use LC/MS successfully. Following a thorough explanation of the basic components and operation of the LC/MS system, the author presents empirical methods for optimizing the techniques, maintaining the instrumentation, and choosing the appropriate MS or LC/MS analyzer for any given problem. LC/MS covers everything users need to know about:The latest equipment, including quadrupole, time-of-flight, and ion trap analyzersCutting-edge processes, such as preparing HPLC mobile phases and samples; handling and maintaining a wide variety of silica, zirconium, and polymeric separation columns; interpreting and quantifying mass spectral data; and using MS interfacesCurrent and future applications in the pharmaceutical and agrochemical industries, biotechnology, clinical research, environmental studies, and forensicsAn accompanying PowerPoint® slide-set on CD-ROM provides vital teaching tools for instructors and new equipment operators. Abundantly illustrated and easily accessible, the text is designed to help students and practitioners acquire optimum proficiency in this powerful and rapidly advancing analytical application.
1Introduction to LC/MS12The HPLC system93The HPLC column and separation modes214HPLC and column maintenance335Sample preparation and separations development416LC/MS interfaces517LC/MS overview598Mass analyzers719Mass spectrometer maintenance8510Application areas for LC/MS9511Trace analysis and LC/MS/MS10312Drug discovery and benchtop LC/MS11113Proteomics : LC/MALDI/TOF and MS/MS libraries11914The future of LC/MS127AppSolvents and volatile buffers for LC/MS
\ From the Publisher"In LC/MS: A Practical User's Guide, the author sets out to introduce LC/MS and provide some practical information for using it ... The present offering seeks to provide a practical resource for LC/MS in 150 pages ... The HPLC chapters will serve the beginning technician Well." (J Am Soc Mass Spectrom, 2011)\ \ \
